Melting Point Apparatus
Addition Funnels
Balances
Chromatography Columns
Condensers
Dean-Stark Apparatus
Desiccators
Distillation Receivers
Filtration
Flasks
Fractionating Columns
Lab Jacks
Manometers
Melting Point Apparatus
Pipettes
Rotary Evaporator
Separating Funnels
Soxhlet Extractor
Still Heads
Stoppers and Adapters
Volumetric Analysis
The simplest method of measuring a melting point is by use of an oil bath (1). A round bottomed flask is partly filled with a mineral oil and the capillary tube containing the sample is attached to a thermometer with a rubber band. The oil is carefully heated with a microburner. The heated block apparatus (2) can be found in many shapes and sizes but the principle is the same; the sample is heated placed in an electrically heated block and the observations are made through a magnified port. The 'hot-stage' apparatus (3) allows the observer to look at the sample through a microscope while its temperature is increased.